Ultrafast scanning of exchangeable sites by NMR spectroscopy

Xiang Xu; Jae Seung Lee; Alexej Jerschow

doi:10.1002/anie.201303255

Ultrafast scanning of exchangeable sites by NMR spectroscopy

Xiang Xu, Jae Seung Lee, Alexej Jerschow

Research output: Contribution to journal › Article › peer-review

41 Scopus citations

Abstract

Development of NMR methods: A fast method is reported to obtain Z-spectra for studying magnetization transfer and chemical exchange saturation transfer phenomena in homogeneous systems. The method exploits gradient fields to irradiate a given system and to acquire the z polarization of water protons simultaneously at many frequency offsets (see picture).

Original language	English (US)
Pages (from-to)	8281-8284
Number of pages	4
Journal	Angewandte Chemie - International Edition
Volume	52
Issue number	32
DOIs	https://doi.org/10.1002/anie.201303255
State	Published - Aug 5 2013
Externally published	Yes

Keywords

NMR spectroscopy
chemical exchange saturation transfer
magnetization transfer
structure elucidation

ASJC Scopus subject areas

Catalysis
Chemistry(all)

Access to Document

10.1002/anie.201303255

Cite this

@article{7d1bfb56106a4c5ba2d0aa21418fe497,

title = "Ultrafast scanning of exchangeable sites by NMR spectroscopy",

abstract = "Development of NMR methods: A fast method is reported to obtain Z-spectra for studying magnetization transfer and chemical exchange saturation transfer phenomena in homogeneous systems. The method exploits gradient fields to irradiate a given system and to acquire the z polarization of water protons simultaneously at many frequency offsets (see picture).",

keywords = "NMR spectroscopy, chemical exchange saturation transfer, magnetization transfer, structure elucidation",

author = "Xiang Xu and Lee, {Jae Seung} and Alexej Jerschow",

year = "2013",

month = aug,

day = "5",

doi = "10.1002/anie.201303255",

language = "English (US)",

volume = "52",

pages = "8281--8284",

journal = "Angewandte Chemie - International Edition",

issn = "1433-7851",

publisher = "John Wiley and Sons Ltd",

number = "32",

}

TY - JOUR

T1 - Ultrafast scanning of exchangeable sites by NMR spectroscopy

AU - Xu, Xiang

AU - Lee, Jae Seung

AU - Jerschow, Alexej

PY - 2013/8/5

Y1 - 2013/8/5

N2 - Development of NMR methods: A fast method is reported to obtain Z-spectra for studying magnetization transfer and chemical exchange saturation transfer phenomena in homogeneous systems. The method exploits gradient fields to irradiate a given system and to acquire the z polarization of water protons simultaneously at many frequency offsets (see picture).

AB - Development of NMR methods: A fast method is reported to obtain Z-spectra for studying magnetization transfer and chemical exchange saturation transfer phenomena in homogeneous systems. The method exploits gradient fields to irradiate a given system and to acquire the z polarization of water protons simultaneously at many frequency offsets (see picture).

KW - NMR spectroscopy

KW - chemical exchange saturation transfer

KW - magnetization transfer

KW - structure elucidation

UR - http://www.scopus.com/inward/record.url?scp=84882265183&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84882265183&partnerID=8YFLogxK

U2 - 10.1002/anie.201303255

DO - 10.1002/anie.201303255

M3 - Article

C2 - 23813633

AN - SCOPUS:84882265183

SN - 1433-7851

VL - 52

SP - 8281

EP - 8284

JO - Angewandte Chemie - International Edition

JF - Angewandte Chemie - International Edition

IS - 32

ER -

Ultrafast scanning of exchangeable sites by NMR spectroscopy

Abstract

Keywords

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this