TY - JOUR
T1 - Principles and applications of a research-oriented gas chromatography-mass spectrometry data system
AU - Campana, J. E.
AU - Risby, T. H.
AU - Jurs, P. C.
N1 - Funding Information:
This work was supported by a grant from the U .S . Environmental Protection Agency (Grant R-80365 ) . We thank E . I . DuPont de Nemours and Co . for donation of a computer graphics system and W . E . Brugger, M . A . Henry, D . E . Klees, A . L . McIntosh, and J . A . Yergey for their contributions in the development of the data system . The MODCOMP /25 computer system was purchased with the partial financial support of the National Science Foundation .
Copyright:
Copyright 2014 Elsevier B.V., All rights reserved.
PY - 1979/12/15
Y1 - 1979/12/15
N2 - A research-oriented gas chromatography-mass spectrometry data system for a quadrupole mass spectrometer has been developed based on a centrally located departmental computer facility. An overview of the hardware and software system is presented, emphasizing the important aspects of on-line computer data acquisition and control and the design philosophy used in the development of the system. The application of the system is demonstrated by the g.c.-m.s. analysis of a mixture of four transition metal β-diketonates (Al, Cr, Rh, and Ru tris-1,1,1-trifluoro-pentane-2,4-dionate). This analysis involved vacuum gas chromatography with a support-coated open tubular column and detection of the eluent by chemical ionization mass spectrometry. The results demonstrate the data system capabilities and indicate the utility of the combined methodologies.
AB - A research-oriented gas chromatography-mass spectrometry data system for a quadrupole mass spectrometer has been developed based on a centrally located departmental computer facility. An overview of the hardware and software system is presented, emphasizing the important aspects of on-line computer data acquisition and control and the design philosophy used in the development of the system. The application of the system is demonstrated by the g.c.-m.s. analysis of a mixture of four transition metal β-diketonates (Al, Cr, Rh, and Ru tris-1,1,1-trifluoro-pentane-2,4-dionate). This analysis involved vacuum gas chromatography with a support-coated open tubular column and detection of the eluent by chemical ionization mass spectrometry. The results demonstrate the data system capabilities and indicate the utility of the combined methodologies.
UR - http://www.scopus.com/inward/record.url?scp=49249146984&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=49249146984&partnerID=8YFLogxK
U2 - 10.1016/S0003-2670(01)85032-7
DO - 10.1016/S0003-2670(01)85032-7
M3 - Article
AN - SCOPUS:49249146984
SN - 0003-2670
VL - 112
SP - 321
EP - 340
JO - Analytica Chimica Acta
JF - Analytica Chimica Acta
IS - 4
ER -